#FILE:080911Cs2TiNb6O18-2.ds1 #FORMAT:NETZSCH5 #IDENTITY:080911-Cs2TiNb6O18-2 #DECIMAL:POINT #SEPARATOR:SEMICOLON #MTYPE:DTA #INSTRUMENT:NETZSCH STA 449F1 #PROJECT:University of Birmingham #DATE/TIME:01/09/2011 10:24:09 #CORR. FILE:10K_O2_Al2O3_lids_correction_30082011.bs1 #LABORATORY:Chemistry #OPERATOR:University of Birmingham #REMARK: #SAMPLE:080911-Cs2TiNb6O18-2 #SAMPLE MASS /mg:44.8 #MATERIAL:Powder #REFERENCE: #REFERENCE MASS /mg:60.3 #TYPE OF CRUCIBLE:DTA/TG crucible Al2O3 #SAMPLE CRUCIBLE MASS /mg:0 #REFERENCE CRUCIBLE MASS /mg:0 #PROTECTIVE GAS:NITROGEN #FLOW RATE: #PURGE GAS 1:OXYGEN #FLOW RATE 1: #PURGE GAS 2:NITROGEN #FLOW RATE 2: #CORR. CODE:020 #EXO:-1 #RANGE:38/10.0(K/min)/1200 #SEGMENT:S1/1 ##Temp./øC;Time/min;_unknown_/(mW/mg);Mass/%;Sensit./(æV/mW) 40.33052;0.0000e+000; 1.2005e-002;100.00000;0.25814 42.83052; 2.84879; 5.3818e-004;100.41744;0.25881 45.33052; 3.56357; 9.1407e-004;100.40378;0.25949 47.83052; 4.08620;-1.5254e-003;100.41279;0.26016 50.33052; 4.51456;-6.6908e-003;100.41056;0.26082 52.83052; 4.88509;-1.4261e-002;100.40956;0.26149 55.33052; 5.21767;-2.3309e-002;100.41068;0.26215 57.83052; 5.52141;-3.4494e-002;100.40354;0.26281 60.33052; 5.80208;-4.6177e-002;100.40547;0.26347 62.83052; 6.06541;-5.8158e-002;100.39733;0.26413 65.33052; 6.31487;-7.1121e-002;100.39242;0.26478 67.83052; 6.55208;-8.7074e-002;100.39053;0.26543 70.33052; 6.77961;-9.9762e-002;100.38106;0.26607 72.83052; 6.99925; -0.11607;100.37908;0.26672 75.33052; 7.21187; -0.13196;100.37340;0.26736 77.83052; 7.41875; -0.14813;100.36572;0.26799 80.33052; 7.62010; -0.16491;100.36285;0.26863 82.83052; 7.81713; -0.18150;100.34968;0.26926 85.33052; 8.00942; -0.19853;100.34275;0.26989 87.83052; 8.19770; -0.21484;100.33167;0.27051 90.33052; 8.38258; -0.23110;100.32561;0.27113 92.83052; 8.56413; -0.24759;100.31476;0.27175 95.33052; 8.74254; -0.26467;100.30100;0.27237 97.83052; 8.91882; -0.28067;100.28716;0.27298 100.33052; 9.09320; -0.29590;100.27335;0.27359 102.83052; 9.26570; -0.31103;100.25768;0.27420 105.33052; 9.43696; -0.32570;100.23977;0.27480 107.83052; 9.60687; -0.34067;100.21815;0.27540 110.33052; 9.77614; -0.35492;100.19076;0.27600 112.83052; 9.94467; -0.36878;100.16849;0.27659 115.33052; 10.11243; -0.38101;100.14059;0.27718 117.83052; 10.27980; -0.39323;100.10626;0.27777 120.33052; 10.44690; -0.40477;100.07553;0.27835 122.83052; 10.61340; -0.41663;100.03605;0.27893 125.33052; 10.77989; -0.42650; 99.99958;0.27950 127.83052; 10.94604; -0.43597; 99.95641;0.28008 130.33052; 11.11191; -0.44494; 99.90548;0.28065 132.83052; 11.27766; -0.45327; 99.85628;0.28121 135.33052; 11.44338; -0.46122; 99.80663;0.28177 137.83052; 11.60952; -0.46768; 99.74948;0.28233 140.33052; 11.77563; -0.47495; 99.68662;0.28289 142.83052; 11.94202; -0.48150; 99.61944;0.28344 145.33052; 12.10914; -0.48705; 99.54828;0.28399 147.83052; 12.27695; -0.49254; 99.49845;0.28453 150.33052; 12.44539; -0.49799; 99.42854;0.28507 152.83052; 12.61483; -0.50271; 99.35701;0.28561 155.33052; 12.78508; -0.50766; 99.28220;0.28614 157.83052; 12.95649; -0.51158; 99.20271;0.28667 160.33052; 13.12919; -0.51545; 99.12110;0.28720 162.83052; 13.30345; -0.52031; 99.04509;0.28772 165.33052; 13.47920; -0.52533; 98.94476;0.28824 167.83052; 13.65624; -0.52925; 98.85082;0.28875 170.33052; 13.83492; -0.53348; 98.76455;0.28926 172.83052; 14.01540; -0.53862; 98.67681;0.28977 175.33052; 14.19778; -0.54357; 98.58767;0.29027 177.83052; 14.38196; -0.54840; 98.49015;0.29077 180.33052; 14.56779; -0.55447; 98.40414;0.29126 182.83052; 14.75561; -0.56021; 98.31865;0.29175 185.33052; 14.94575; -0.56690; 98.22420;0.29224 187.83052; 15.13799; -0.57231; 98.12864;0.29272 190.33052; 15.33239; -0.57909; 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95.59588;0.31725 402.83052; 36.63852; -1.16844; 95.59097;0.31733 405.33052; 36.88861; -1.17632; 95.58810;0.31740 407.83052; 37.13882; -1.18500; 95.58523;0.31747 410.33052; 37.38901; -1.19371; 95.58885;0.31754 412.83052; 37.63906; -1.20272; 95.59026;0.31760 415.33052; 37.88926; -1.21334; 95.58447;0.31765 417.83052; 38.13886; -1.22469; 95.58366;0.31770 420.33052; 38.38862; -1.23555; 95.58475;0.31774 422.83052; 38.63877; -1.24795; 95.58104;0.31778 425.33052; 38.88937; -1.26005; 95.58054;0.31781 427.83052; 39.13946; -1.27345; 95.58103;0.31784 430.33052; 39.38993; -1.28662; 95.58036;0.31786 432.83052; 39.64010; -1.29996; 95.57829;0.31788 435.33052; 39.89032; -1.31427; 95.58136;0.31790 437.83052; 40.14068; -1.32828; 95.58275;0.31790 440.33052; 40.39106; -1.34258; 95.57965;0.31791 442.83052; 40.64121; -1.35626; 95.57836;0.31790 445.33052; 40.89147; -1.37023; 95.57989;0.31790 447.83052; 41.14168; -1.38577; 95.58071;0.31788 450.33052; 41.39209; -1.40107; 95.58128;0.31786 452.83052; 41.64201; -1.41547; 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